HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 21163158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 21163151 | HCID 21163151 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21163158 | HCID 21163158 | 72.8% |
Reaction Steps
Methyl 3-[7-benzyl-4-oxo-8-propyl-4H-1-benzopyran-2-yl]propionate (1.0 g) was refluxed with ethanol (50 ml) containing 10% aqueous sodium carbonate solution (10 ml) for 30 minutes. The mixture was diluted with water, washed with ethyl acetate, and acidified to give a solid, which crystallised from ethanol to give the propionic acid (0.7 g), mp 160°-161°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04281008 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-03d5c5690a4843ceb0e71d6cc9a6f612 |
| Source note | uspto-grants-1981_07 |