HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lactic Acid → 1-Carboxyethyl 4-(15-carbomethoxypentadecylamino)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lactic Acid | HCID 612 | — |
| Reactant | 2-Methylbenzenesulfonic acid | HCID 6925 | — |
| Reactant | p-(15-Carbomethoxypentadecylamino)benzoic acid | HCID 12898273 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 1-Carboxyethyl 4-(15-carbomethoxypentadecylamino)benzoate | HCID 21163344 | — |
Reaction Steps
A flask containing 10.0 g. 4-(15-carbomethoxypentadecylamino)benzoic acid, 3.3 g. lactic acid, 500 mg. toluenesulfonic acid and 500 ml. toluene is equipped with a Soxhlet extractor charged with activated 4 A Linde molecular sieves. The solution is refluxed for 4 hours, during which time the Soxhlet extractor is charged twice more with fresh sieves. The hot solution is filtered and left to cool, whereupon the product separates as off-white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04281018 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-afe0204fbdfb4bae9cbeecedde01d34b |
| Source note | uspto-grants-1981_07 |