HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2,6-diethylaniline → HCID 18430566, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2,6-diethylaniline | HCID 597855 | — |
| Reactant | HCID 13799153 | HCID 13799153 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 18430566 | HCID 18430566 | — |
Reaction Steps
In 100 ml of tetrahydrofuran was dissolved 8.0 g (39.4 mmol) of 1-methyl-pyrazolo[5,4-b]pyridine-5,6-dicarboxylic acid anhydride. After adding 7.23 g (39.4 mmol) of 3-chloro-2,6-diethylaniline to the solution obtained above, a reaction was carried out at ambient temperature for 12 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06444617B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-56c820da36d94950ae67e259067d62d0 |
| Source note | uspto-grants-2002_09 |