3-Chloro-2,6-diethylaniline → HCID 18430566, compound

HRID 1278545Notes

Reaction equation

HRID 1278545 reaction equation
[CH3:1][N:2]1[C:6]2=[N:7][C:8]3[C:14](=[O:15])[O:13][C:11](=[O:12])[C:9]=3[CH:10]=[C:5]2[CH:4]=[N:3]1.[Cl:16][C:17]1[C:18]([CH2:26][CH3:27])=[C:19]([C:21]([CH2:24][CH3:25])=[CH:22][CH:23]=1)[NH2:20]>O1CCCC1>[Cl:16][C:17]1[C:18]([CH2:26][CH3:27])=[C:19]([NH:20][C:14]([C:8]2[N:7]=[C:6]3[N:2]([CH3:1])[N:3]=[CH:4][C:5]3=[CH:10][C:9]=2[C:11]([OH:13])=[O:12])=[O:15])[C:21]([CH2:24][CH3:25])=[CH:22][CH:23]=1

Participants

4

Reactant 2

HCID 5978553-Chloro-2,6-diethylanilineHCID 13799153HCID 13799153, compound

Product 1

HCID 18430566HCID 18430566, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

In 100 ml of tetrahydrofuran was dissolved 8.0 g (39.4 mmol) of 1-methyl-pyrazolo[5,4-b]pyridine-5,6-dicarboxylic acid anhydride. After adding 7.23 g (39.4 mmol) of 3-chloro-2,6-diethylaniline to the solution obtained above, a reaction was carried out at ambient temperature for 12 hours.

Workup

  1. customobtained above, a reaction

Sources & evidence

ORD record
ord-56c820da36d94950ae67e259067d62d0
Source dataset
uspto-grants-2002_09
Patent number
US06444617B1

Reaction notes

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