CHEBI:5834 → HCID 70148574, compound

Participants

Reaction Steps

23 mg (1 mmol) sodium is dissolved in 50 ml anhydrous methanol. 536 mg (1 mmol) hyperforin is dissolved in this solution under stirring, and the solution evaporated. The residue is dissolved in 100 ml water and lyophilised. Yield: 556 mg of a light-coloured powder (99.6% of theoretical). Mp.: Degradation from 170° C. IR: 1420-1500 cm−(sv).

Provenance & Evidence