HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(6-formyl-1-isoquinolinyl)benzamide → N-(7-Formylisoquinolinyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(6-formyl-1-isoquinolinyl)benzamide | HCID 22665740 | — |
| Reactant | N-(7-bromo-1-isoquinolinyl)benzamide | HCID 22665843 | — |
| Product | N-(7-Formylisoquinolinyl)benzamide | HCID 22665912 | — |
Reaction Steps
N-(7-Formylisoquinolinyl)benzamide was prepared from 37e using the procedure described for 1f but was not purified using column chromatography. The crude aldehyde was transformed into the title compound using the procedure described for 1 g folowed by purification using column chromatography on silica gel (toluene/ethyl acetate:2/1). M.p. 137.5-139.0° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06444672B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-090c2f6d29f0443797bbf76b7d791d42 |
| Source note | uspto-grants-2002_09 |