HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 178477935, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | (5-p-Chlorophenyl-1-phenyl-pyrazol-4-yl)-acetonitrile | HCID 53675380 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178477935 | HCID 178477935 | — |
Reaction Steps
A mixture of 29.4 g of (5-p-chlorophenyl-1-phenyl-pyrazol-4-yl)-acetonitrile, 8.06 g of sodium azide, 6.64 g of NH4Cl and 140 ml of dry DMF is heated at 120° for 17 hours, with stirring, and is then evaporated. After the customary working up, 5-p-chlorophenyl-1-phenyl-4-(tetrazol-5-ylmethyl)-pyrazole is obtained; m.p. 230°-232°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04258047 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-ff26bf1ac36349808214f328ab332ac0 |
| Source note | uspto-grants-1981_03 |