Hydrochloric Acid → HCID 18770379, compound

Participants

Reaction Steps

Concentrated hydrochloric acid (0.025 ml; 0.30 mmol) was added to a solution of 1,3-bis[4-[(E,E)-5-(4-tert-butyl-2-methoxyphenyl)-2,4-pentadienoyl]-1-piperazinyl]-propane (49 mg; 0.070 mmol) in ethanol (5 ml) and the reaction mixture was concentrated under reduced pressure. A process of adding ethanol (10 ml) to the residue and concentrating the mixture under reduced pressure was performed twice to obtain the title compound as a pale yellow amorphous powder.

Provenance & Evidence