Hydrochloric Acid → HCID 18770416, compound

Participants

Reaction Steps

Concentrated hydrochloric acid (0.040 ml; 0.48 mmol) was added to a solution of 1,3-bis[4-[(E,E)-5-(4-trifluoromethylphenyl)-2,4-pentadienoyl]-1-piperazinyl]propane (111 mg; 0.16 mmol) in ethanol (5 ml) and the reaction mixture was concentrated under reduced pressure. After a process of adding ethanol (10 ml) to the residue and concentrating the mixture under reduced pressure was performed twice, the resultant concentrated residue was recrystallized from ethanol-diethyl ether to obtain the title compound as a colorless crystalline powder.

Provenance & Evidence