Hydrochloric Acid → HCID 18770399, compound

Participants

Reaction Steps

Concentrated hydrochloric acid (0.080 ml; 0.96 mmol) was added to a solution of 2,6-bis[[4-[4-(3,4,5-trimethoxyphenyl)benzoyl]-1-piperazinyl]methyl]pyridine (157 mg; 0.19 mmol) in ethanol (5 ml) and the reaction mixture was concentrated under reduced pressure. After a process of adding ethanol (10 ml) to the residue and concentrating the mixture under reduced pressure was performed twice, the resultant concentrated residue was recrystallized from methanol-diethyl ether to obtain the title compound as a colorless crystalline powder.

Provenance & Evidence