HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 178425252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | 7-Methoxy-3,3-dimethyl-2,4,5,6-tetrahydroazepine | HCID 18428605 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178425252 | HCID 178425252 | 91.3% |
Reaction Steps
The product of EXAMPLE 63 (490 mg, 3.2 mmol) in 18 mL of MeOH was reacted with ammonium chloride (125 mg, 2.4 mmol) by the method of EXAMPLE 27 to yield 387 mg (69%) of the title material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06448286B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-e16a8d69d77948c4a532ff1e6e89c2d5 |
| Source note | uspto-grants-2002_09 |