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HRID127951

反应详情

EQUATION

反应方程式

HRID 127951 的结构方程式

REACTANTS

反应物

2
结构：CN=C=O
HCID12228

Methyl isocyanate

C2H3NO

结构：CC(C)(C)NCC(O)C(Cl)(Cl)Cl
HCID23471020

未命名化合物

PRODUCTS

生成物

2
结构：CNC(=O)N(CC(O)C(Cl)(Cl)Cl)C(C)(C)C
HCID23471018

未命名化合物

结构：CNC(=O)OC(CN(C(=O)NC)C(C)(C)C)C(Cl)(Cl)Cl
HCID23471019

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

The reaction of 3-(1,1-dimethylethylamino)-1,1,1-trichloro-2-propanol with methyl isocyanate normally takes place at -70° to +80° C. in an inert solvent such as chloroform to produce 1-(1,1-dimethylethyl)-3-methyl-1-(3,3,3-trichloro-2-hydroxypropyl)urea and 1-(1,1-dimethylethyl)-3-methyl-1-[3,3,3-trichloro-2-(methylcarbamoyloxy)propyl]urea.