Dimethyl Sulfate → HCID 12604432, compound

HRID 1279512Notes

Reaction equation

HRID 1279512 reaction equation
[C:1]([CH:5]1[CH2:12][CH2:11][NH:10][C:8](=[O:9])[CH2:7][CH2:6]1)([CH3:4])([CH3:3])[CH3:2].[CH3:13]OS(OC)(=O)=O>>[CH3:3][C:1]([CH:5]1[CH2:6][CH2:7][C:8]([O:9][CH3:13])=[N:10][CH2:11][CH2:12]1)([CH3:4])[CH3:2]

Participants

3

Reactant 2

HCID 6497Dimethyl SulfateHCID 984324-tert-Butylcaprolactam

Product 1

HCID 12604432HCID 12604432, compound

Procedure

A sample of 4-tertbutylcaprolactam (Bader, 2.5 g, 14.8 mmol) was reacted with dimethylsulfate (1.4 mL, 14.8 mmol) by the method of EXAMPLE 69 to yield, after chromatography, 2.7 g of the title material.

Workup

  1. customto yield

Sources & evidence

ORD record
ord-f75071396641490fbc8206b10213a0b7
Source dataset
uspto-grants-2002_09
Patent number
US06448286B1

Reaction notes

Loading…