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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1279512Generated: November 1, 2026

Dimethyl Sulfate → HCID 12604432, compound

https://huagongshe.com/reaction/1279512

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethyl SulfateHCID 6497—
Reactant4-tert-ButylcaprolactamHCID 98432—
ProductHCID 12604432HCID 12604432—

Reaction Steps

A sample of 4-tertbutylcaprolactam (Bader, 2.5 g, 14.8 mmol) was reacted with dimethylsulfate (1.4 mL, 14.8 mmol) by the method of EXAMPLE 69 to yield, after chromatography, 2.7 g of the title material.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06448286B1
Source datasetuspto-grants-2002_09
ORD IDord-f75071396641490fbc8206b10213a0b7
Source noteuspto-grants-2002_09