HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3,4,5-Tetrahydro-2H-1-benzazepin-2-one → HCID 18428530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3,4,5-Tetrahydro-2H-1-benzazepin-2-one | HCID 248580 | — |
| Reactant | Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) | HCID 2735153 | — |
| Product | HCID 18428530 | HCID 18428530 | — |
Reaction Steps
A sample of the title compound of EXAMPLE 165 (3.2 g, 20.0 mmol) was reacted with trimethyloxonium tetrafluoroborate (4.4 g, 30.0 mmol) by the method of EXAMPLE 26 to yield, after chromatography, 2.5 g (73%) of the title material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06448286B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-6f62db7a5912451082df819a0bde9a3d |
| Source note | uspto-grants-2002_09 |