HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → N-(1,1-dimethylethyl)-N-(3,3,3-trichloro-2-hydroxypropyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 3-(Tert-butylamino)-1,1,1-trichloropropan-2-ol | HCID 23471020 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-(1,1-dimethylethyl)-N-(3,3,3-trichloro-2-hydroxypropyl)acetamide | HCID 23471021 | — |
Reaction Steps
The reaction of 3-(1,1-dimethylethylamino)-1,1,1-trichloro-2-propanol with acetic anhydride takes place at about -70° to +70° C. in a solvent such as dichloromethane to produce the N-(1,1-dimethylethyl)-N-(3,3,3-trichloro-2-hydroxypropyl)acetamide of this invention.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04258060 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-b464da8834294a5189355b6d91486acd |
| Source note | uspto-grants-1981_03 |