HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → 4-Methyl-5-(2-propenyl)pyrrolidin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 5-(3-Hydroxypropyl)-4-methylpyrrolidin-2-one | HCID 18428563 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 4-Methyl-5-(2-propenyl)pyrrolidin-2-one | HCID 18782103 | — |
Reaction Steps
The product of EXAMPLE 235 is treated with PTSA in refluxing toluene, with a Dean-Stark trap to remove water. The solvent is removed to yield the title material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06448286B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-cf10568937ee4306b9b4bd20cf50ee67 |
| Source note | uspto-grants-2002_09 |