HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Propylpyridin-2-amine → HCID 178476207, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Propylpyridin-2-amine | HCID 7022594 | — |
| Reactant | 2-Imino-4-methylpiperidine acetate | HCID 178475870 | — |
| Product | HCID 178476207 | HCID 178476207 | — |
Reaction Steps
The method of preparation of 2-imino-4-methylpiperidine acetate was used to convert 2-amino-4-(n-propyl)pyridine to the title compound except platinum oxide was used as the catalyst. Product was triturated with EtOAc to give a white solid. The analysis of the product was found to be consistent with the proposed structure. MH+141; 1H NMR (D2O): δ63.35-3.05 (m, 2H); 2.60-2.40 (m, 1H); 2.15-2.00 (m, 1H); 1.80-1.60 (m, 2H); 1.78 (s, 3H); 1.35-1.05 (m, 5H); 0.75-0.65 (m, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06448286B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-32d58ddcce4f444396d2c71eb8286903 |
| Source note | uspto-grants-2002_09 |