HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzenesulfonyl chloride → HCID 23470966, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzenesulfonyl chloride | HCID 7398 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 23470963 | HCID 23470963 | — |
| Product | HCID 23470966 | HCID 23470966 | 32% |
Reaction Steps
By the reaction of 2-[4-(2-aminoethyl)-phenoxy]-n-hexanoic acid with 4-chlorobenzenesulphonyl chloride in the presence of aqueous potassium carbonate solution, in a manner analogous to that described in Example 1, there is obtained a yield of 32% of theory of 2-{4-[2-(4-chlorobenzenesulphonylamino)-ethyl]-phenoxy}-n-hexanoic acid; m.p. 138°-139° C. (recrystallized from ethyl acetate and cyclohexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04258058 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-29b41d65b70e41adb45c55c1abc9964f |
| Source note | uspto-grants-1981_03 |