反应详情

Following the procedure described in example 1 [step (c)], tetrahydrofluorene (17.6 mmol), butyllithium (11 ml of a solution 1.6M in hexane, 17.6 mmol) and dichlorodimethylsilane (1.07 ml, 8.81 mmol) gave a yellow oil.

1. customgave a yellow oil