HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichlorodimethylsilane → HCID 66589487, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichlorodimethylsilane | HCID 6398 | — |
| Reactant | 2,3,4,9-Tetrahydro-1H-fluorene | HCID 588465 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 66589487 | HCID 66589487 | — |
Reaction Steps
Following the procedure described in example 1 [step (c)], tetrahydrofluorene (17.6 mmol), butyllithium (11 ml of a solution 1.6M in hexane, 17.6 mmol) and dichlorodimethylsilane (1.07 ml, 8.81 mmol) gave a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06448424B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-9f0ef7c4a59a4ae1b57f5ef1d6d90708 |
| Source note | uspto-grants-2002_09 |