HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18429306, compound → HCID 18429151, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18429306 | HCID 18429306 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Palladium | HCID 23938 | — |
| Product | HCID 18429151 | HCID 18429151 | — |
Reaction Steps
3,5-Dinitro-(2-hydroxyethyl)benzene (0.18 g, 0.85 mmol) was dissolved in methanol (50 ml) and hydrogenated over Pd/C (10%) in a Parr apparatus at 60 psi. After complete hydrogen uptake the catalyst was filtered off and the solvent was evaporated which gave a solid residue of 0.10 g (81%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06448442B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-da8f3045891b45528f9ef4479f69fe1f |
| Source note | uspto-grants-2002_09 |