HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetoxyacetyl chloride → HCID 86757557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetoxyacetyl chloride | HCID 26297 | — |
| Reactant | HCID 18429197 | HCID 18429197 | — |
| Solvent | Acetonitrile methylene chloride | HCID 21877088 | — |
| Product | HCID 86757557 | HCID 86757557 | 64% |
Reaction Steps
The product in Example 64e, 3,5-diamino-2,4,6-triiodo-(2,3-diacetoxypropyl)benzene was acylated using acetoxyacetyl chloride according to the general procedure in Example 24i. After chromatography on silica gel using methylene chloride/acetonitrile (3/1) as the eluent the product was isolated in 64% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06448442B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-430d5a88f1164a9080d1914ef5773612 |
| Source note | uspto-grants-2002_09 |