HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 54053566, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 19361980 | HCID 19361980 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54053566 | HCID 54053566 | — |
Reaction Steps
0.5 ml of dimethylformamide and 60.9 g (0.48 mol) of oxalyl chloride were added to a solution of 37.3 g (0.16 mol) of 2,3-dichloro-4-methoxyphenylacetic acid in 0.5 l of dichloromethane. After evolution of gas had ceased (about 2 hours), the mixture was concentrated. The crude product was reacted further in the next step without any purification. Yield: quantitative.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451734B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-f4c3c8c2690b4f27a8a3b6ab38079074 |
| Source note | uspto-grants-2002_09 |