Ethanol → HCID 23471632, compound

Participants

Reaction Steps

A solution of 10.0 g (0.285 mole) of 1-(2-benzoyl-4-chlorophenyl)-3-phenylurea in 50 ml ethanol was refluxed for 18 hr, and then cooled. The solid that formed was collected on a filter and washed with ethanol to give 9.46 g (88%) of 6-chloro-4-ethoxy-3,4-dihydro-3,4-diphenyl-2(1H)-quinazolinone as colorless crystals: mp 209°-211°. The 1H nmr spectrum shows the presence of an ethyl group in addition to aromatic hydrogens.

Provenance & Evidence