反应详情

To a solution of 6 (0.43 g, 2.3 mmol) in ethanol(4 ml) was added 5 (0.405 g, 1.64 mmol). The solution was heated to reflux and stirred for 24 h. Upon completion the solution was concentrated in vacuo and purified using Prep TLC (10:1, DCM:MeOH) to yield 7. Mass Spectrum (M+1)=438.36.

1. temperatureThe solution was heated
2. temperatureto reflux
3. concentrationUpon completion the solution was concentrated in vacuo
4. custompurified
5. customto yield 7