HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formamidine acetate → HCID 17904467, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formamidine acetate | HCID 160693 | — |
| Reactant | N-(4-Nitrophenyl)hydrazinecarboxamide | HCID 12467017 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 17904467 | HCID 17904467 | — |
Reaction Steps
A mixture of intermediate (2) and methanimidamide acetate (2.4 mol) in 1-butanol (1500 ml) was stirred and refluxed for 5 hours and then stirred further for 48 hours. The precipitate was filtered off and washed with DIPE, yielding 48 g of 2,4-dihydro-4-(4-nitrophenyl) -3H-1,2,4-triazol-3-one (intermediate 3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451802B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-84a9d729e8fb461e9eddd7cdbf18b0d7 |
| Source note | uspto-grants-2002_09 |