HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20436151, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-Pentenoic acid | HCID 61138 | — |
| Reactant | Hydroxylamine, sulfate (1:1) | HCID 159255 | — |
| Reactant | HCID 54113944 | HCID 54113944 | — |
| Reactant | HCID 73678918 | HCID 73678918 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20436151 | HCID 20436151 | — |
Reaction Steps
Reaction of 3,3-dimethyl-12-n-hexyl-1-aza-1,5,9-cyclododecatriene with hydroxylamine sulfate, in the presence of hydrochloric acid and water, to 2,2-dimethyl-11-n-hexyl-11-amino-undeca-4,8-dienal-oxime, and hydrogenation of this to given 1-n-hexyl-10,10-dimethyl-1,10-diaminoundecane; b.p. 135° C./4 Pa; nD20 =1.4624.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04258176 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-2a99b935046a4e5c8b0036b48882fd8f |
| Source note | uspto-grants-1981_03 |