HRID128049

反应详情

EQUATION

反应方程式

HRID 128049 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Reaction of 3,3-dimethyl-12-n-hexyl-1-aza-1,5,9-cyclododecatriene with hydroxylamine sulfate, in the presence of hydrochloric acid and water, to 2,2-dimethyl-11-n-hexyl-11-amino-undeca-4,8-dienal-oxime, and hydrogenation of this to given 1-n-hexyl-10,10-dimethyl-1,10-diaminoundecane; b.p. 135° C./4 Pa; nD20 =1.4624.