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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1280760Generated: November 2, 2026

Oxalyl chloride → HCID 54045789, compound

https://huagongshe.com/reaction/1280760

Reaction equation

Participants

RoleNameHCIDCharge
ReactantOxalyl chlorideHCID 65578—
Reactant3-(3-Pyridinyl)-2-propenoic acidHCID 101984—
ReactantHCID 15390853HCID 15390853—
ProductHCID 54045789HCID 54045789—

Reaction Steps

Batch size: 2.6 g (17.6 mmol) 3-(3-pyridyl)-acrylic acid, 2.6 g (20.8 mmol) oxalyl chloride and 5.57 g (16.0 mmol) 4-[1-(10,11-dihydro-5H-dibenzo[a,d]cycloheptene-5-yl)-piperidin-4-yl]-butylamine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06451816B1
Source datasetuspto-grants-2002_09
ORD IDord-f22e1d1715f84d6fa2b061e0c0b44100
Source noteuspto-grants-2002_09