HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl carbazate → HCID 56980124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Reactant | 5-Methoxyindan-1-one | HCID 78787 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 56980124 | HCID 56980124 | — |
Reaction Steps
A solution of 5-methoxyindan-1-one (5.46 g) and tert-butyl carbazate (4.45 g) in ethanol (100 ml) and glacial acetic acid (1 drop) was stirred and boiled under reflux for 2 hours. The volume was reduced by half under reduced pressure and the solid which crystallized was collected by filtration to give 5-methoxyindan-1-one tert-butyloxycarbonylhydrazone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451834B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-ef1cc3033e1b4cc0bdd499caa7ec3f76 |
| Source note | uspto-grants-2002_09 |