HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Indanone → HCID 57072976, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Indanone | HCID 6735 | — |
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57072976 | HCID 57072976 | — |
Reaction Steps
A solution of indan-1-one (5.0 g) and tert-butyl carbazate (5.0 g) in methanol (20 ml) containing glacial acetic acid (1 drop) was boiled and stirred under reflux for 1.5 hours. The mixture was cooled and evaporated under reduced pressure. The residue was recrystallized from ethanol to give indan-1-one tert-butyloxycarbonyl-hydrazone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451834B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-b4a076868f2841238a0b1733acdd9373 |
| Source note | uspto-grants-2002_09 |