HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 9885552, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 12015899 | HCID 12015899 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 9885552 | HCID 9885552 | 46.1% |
Reaction Steps
A solution of [[2-ethyl-1-(phenylmethyl)-3-ureido-1H-indol-4-yl]oxy]acetic acid tert-butyl ester (0.2 g) and trifluoroacetic acid (0.3 mL) in 5 mL of methylene chloride was stirred at room temperature for 18 hours. After concentrating to dryness, the resulting solid was slurried in ether, filtered and air dried to give 0.08 g of titled compound. Mass spectrum: 368.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451839B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-180ffc2ce88647bca74589abc746d926 |
| Source note | uspto-grants-2002_09 |