HRID1280818

反应详情

EQUATION

反应方程式

HRID 1280818 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

(2-Phenyl)-phenylmethyl bromide (6 g, 0.0243 mol) and potassium phthalimide (5 g, 0.0270 mol) were mixed together in dimethyl formamide at room temperature, stirred for 60 hrs, diluted with cold water, and the solid isolated by filtration. After washing with water, isopropyl alcohol, and hexane the white solid was vacuum dried to yield 6.9 g of the subtitled compound. Mass spectrum: 313

WORKUP

后处理

  1. customthe solid isolated by filtration
  2. washAfter washing with water, isopropyl alcohol, and hexane the white solid
  3. customdried