Hydrochloric Acid → HCID 12361798, compound

HRID 128105Notes

Reaction equation

HRID 128105 reaction equation
Cl.Cl.[CH3:3][N:4]([CH3:20])[CH:5]1[CH2:17][C:16]2[C:15]3[C:10](=[C:11]([CH2:18][CH3:19])[CH:12]=[CH:13][CH:14]=3)[NH:9][C:8]=2[CH2:7][CH2:6]1>CCOCC>[CH3:3][N:4]([CH3:20])[CH:5]1[CH2:17][C:16]2[C:15]3[C:10](=[C:11]([CH2:18][CH3:19])[CH:12]=[CH:13][CH:14]=3)[NH:9][C:8]=2[CH2:7][CH2:6]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 12361799HCID 12361799, compound

Product 1

HCID 12361798HCID 12361798, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Following the procedure given in Example 3 and using 9 g. of 4-dimethylaminocyclohexanone and 11 g. of 2-ethylphenylhydrazine hydrochloride there was obtained, after treatment of the free base in ether with ethereal hydrogen chloride, 6.7 g. of 3-(dimethylamino)-8-ethyl-1,2,3,4-tetrahydrocarbazole hydrochloride, m.p. 282°-285° C.

Sources & evidence

ORD record
ord-244aca7153c241cc8fcb57de633444aa
Source dataset
uspto-grants-1981_03
Patent number
US04257952

Reaction notes

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