HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylethylenediamine → HCID 22664376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylethylenediamine | HCID 66053 | — |
| Reactant | HCID 22664396 | HCID 22664396 | — |
| Product | HCID 22664376 | HCID 22664376 | — |
Reaction Steps
The title compound is prepared according to the procedure given in instant Example 35 using 8.0 g of the intermediate compound prepared in Example 34a and 1.4 g of 2-dimethylaminoethylamine. After several recrystallizations from ethyl acetate and ethyl acetate/heptane mixtures, 5.6 g of the title compound is prepared as a near white solid melting at 118-120° C. The structure of the compound is confirmed by 1Hnmr and mass spectroscopy analyses.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451887B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-22a10c0f50cf46a0b05cafcc1896c46a |
| Source note | uspto-grants-2002_09 |