HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 86746863, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 131722603 | HCID 131722603 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86746863 | HCID 86746863 | — |
Reaction Steps
The compound (16-a)(0.514 g) was dissolved in the solvent mixture (acetic acid:water:THF=4:2:1)(30 ml), and the solution was maintained overnight at room temperature. The titled compound (16-b) was obtained by purifying the crude product on silica gel column [yield:0.272 g(61%)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06452039B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-cb5d905d62624077a8939a8ff49bf356 |
| Source note | uspto-grants-2002_09 |