HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131722604, compound → HCID 70148109, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131722604 | HCID 131722604 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 70148109 | HCID 70148109 | — |
Reaction Steps
The compound (12-9)(1.39 g) was subjected to catalytic reduction in ethyl acetate (15 ml) using 5% Pd—C (0.14 g) under hydrogen atmosphere. The crude product obtained by the conventional treatment was purified by silica gel chromatography (n-hexane/ethyl acetate=8/2) to give the titled compound (12-10).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06452039B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-bcd0bc172163418bb503815b5c9f9a52 |
| Source note | uspto-grants-2002_09 |