HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → Chlorthal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 2,3,5,6-tetrachloro-1,4-benzenedicarboxamide | HCID 11324087 | — |
| Product | Chlorthal | HCID 16493 | — |
Reaction Steps
In the hydrolysis of 2,3,5,6-tetrachloro-1, 4-benzenedicarboxamide, as is apparent from Examples 4 and 5, the maximum reduction of the amount of water in sulfuric acid resulted in efficiently forming desired 2,3,5,6-tetrachloro-1,4-benzenedicarboxylic acid by heating 2,3,5,6-tetrachloro-1,4-benzenedicarboxamide at 180 or 130° C. for 7 or 27 hr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06452046B2 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-cd675f3a0acd4764bca6237d1da57827 |
| Source note | uspto-grants-2002_09 |