Potassium Bromide → HCID 22237613, compound

Participants

Reaction Steps

The title compound was prepared as a white solid (0.559 g, 67%) from (5′-Hexyl-[1,1′;3′,1″]terphenyl-2′-yloxy)acetic acid, methyl ester (0.870 g, 2.161 mmol) using a procedure similar to step 4 of example 165; mp 87-89° C.; 1H NMR (400 MHz, DMSO-d6) δ 0.82-0.86 (m, 3H), 1.22-1.37 (m, 6H), 1.56-1.64 (m, 2H), 2.61 (t, J=7.5 Hz, 2H), 3.71 (s, 2H), 7.16 (s, 2H), 7.32-7.37 (m, 2H), 7.39-7.44 (m, 4H), 7.59 (m, 4H), 12.47 (broad s, 1H); IR (KBr) 3450, 2920, 1725, 1420, 1210 cm−1; mass spectrum [EI], m/z 388 M+; Anal. Calcd. for C26H28O3: C, 80.38; H, 7.26; N, 0.00, Found: C, 79.99; H, 7.24; N, 0.13.

Provenance & Evidence