Carbon Disulfide → HCID 86737623, compound

HRID 128150Notes

Reaction equation

HRID 128150 reaction equation
[Cl:1][C:2]1[CH:13]=[C:12]([Cl:14])[CH:11]=[CH:10][C:3]=1[O:4][CH2:5][C:6]([NH:8][NH2:9])=[O:7].[C:15](=S)=[S:16]>CN(C=O)C>[Cl:1][C:2]1[CH:13]=[C:12]([Cl:14])[CH:11]=[CH:10][C:3]=1[O:4][CH2:5][CH:6]1[N:8]=[N:9][C:15](=[S:16])[O:7]1

Participants

4

Reactant 2

HCID 6348Carbon DisulfideHCID 3123302-(2,4-dichlorophenoxy)acetohydrazide

Product 1

HCID 86737623HCID 86737623, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Following the procedure of Example IIA, 2,4-dichlorophenoxyacetic acid hydrazide (23.5 g) and carbon disulfide (38 g) in DMF (50 ml) were reacted and worked up to yield 2-(2,4-dichlorophenoxymethyl)-1,3,4-oxadiazol-5-thione (IIIA).

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-b764e328b91e4bce8cd9a3685e722144
Source dataset
uspto-grants-1981_03
Patent number
US04259104

Reaction notes

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