HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70132990, compound → HCID 10167042, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70132990 | HCID 70132990 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 10167042 | HCID 10167042 | 56.3% |
Reaction Steps
Methyl 2-{4-[({4-[4-(2-{[(2S)-2-hydroxy-3-(4-{[isopropyl(diphenyl)silyl]oxy}phenoxy)propyl]amino}ethyl)anilino]piperidinyl}carbonyl)amino]phenoxy}acetate (0.16 g, 0.192 mmol) was reacted according to Procedure H (eluant: 10:1 going to 5:1 chloroform-methanol containing 2% triethylamine) to give the title compound (0.64 g, 0.108 mmol)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451814B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-dbbf4715047d4c319a3415c6204e9b4d |
| Source note | uspto-grants-2002_09 |