HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl-(4-oxiranylmethoxy-phenoxy)-diphenylsilane → HCID 10168591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl-(4-oxiranylmethoxy-phenoxy)-diphenylsilane | HCID 12045564 | — |
| Reactant | HCID 70133039 | HCID 70133039 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 10168591 | HCID 10168591 | 29.4% |
Reaction Steps
4-[4-(2-Aminoethyl)anilino]-N-(4-{[(hexylamino)carbonyl]amino}benzyl)-1-piperidinecarboxamide formate (0.29 g, 0.54 mmol) was reacted with tert-butyl-(4-oxiranylmethoxy-phenoxy)-diphenyl-silane (0.220 g, 0.54 mmol) according to Procedure G (eluant: 20:1 going to 10:1 chloroform-methanol) to give the title compound (0.143 g, 0.159 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451814B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-cee94fd6a0634250bd900a6700fb782f |
| Source note | uspto-grants-2002_09 |