HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70029000, compound → HCID 10168591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70029000 | HCID 70029000 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 10168591 | HCID 10168591 | 75.5% |
Reaction Steps
4-[4-(2-{[(2S)-3-(4-{[tert-Butyl(diphenyl)silyl]oxy}phenoxy)-2-hydroxypropyl]amino}ethyl)aniiino]-N-(4-{[(hexylamino)carbonyl]amino}benzyl)-1-piperidinecarboxamide (0.143 g, 0.159 mmol) was reacted according to Procedure H (eluant: 10:1 going to 5:1 chloroform-methanol containing 2% triethylamine) to give the title compound (0.077 g, 0.12 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06451814B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-227ac003843c46cf8ff354bb81c7933f |
| Source note | uspto-grants-2002_09 |