HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 18422197, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 18422373 | HCID 18422373 | — |
| Catalyst | Titanium Tetrachloride | HCID 24193 | — |
| Solvent | Anisole | HCID 7519 | — |
| Product | HCID 18422197 | HCID 18422197 | — |
Reaction Steps
In the same manner as in Example 1 and using ethyl 2-(N-methyl-2-nitroanilino)benzo[b]thiophene-3-carboxylate (3.2 g), 1-methylpiperazine, anisole (80 ml) and titanium tetrachloride (3.5 ml), 6-methyl-12-(4-methylpiperazin-1-yl)[1]benzothieno[2,3-b][1,5]benzodiazepine (166 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455521B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-5dc06eb1e9a84c8fa48a98c93b5818fa |
| Source note | uspto-grants-2002_09 |