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HRID128182

反应详情

EQUATION

反应方程式

HRID 128182 的结构方程式

REACTANTS

反应物

2
结构：CN
HCID6329

Methylamine

CH5N

结构：CON=C(C1=Nc2ccc(Cl)cc2C(c2ccccc2F)=NC1)[N+](=O)[O-]
HCID54384993

未命名化合物

PRODUCTS

生成物

1
结构：CNC(=NOC)C1=Nc2ccc(Cl)cc2C(c2ccccc2F)=NC1
HCID178485194

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Reaction of 0.5 g of 7-chloro-5-(2-fluorophenyl)-N-methoxy-α-nitro-3H-1,4-benzodiazepine-2-methanimine with methylamine in ethanol (20% v/v) gave the same workup and purification procedure colorless product, crystallized from ether/hexane; mp 140°-142° C.

WORKUP

后处理

  1. customgave
  2. customthe same workup and purification procedure colorless product
  3. customcrystallized from ether/hexane