HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Methoxyphenyl)piperazine → HCID 18423158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Methoxyphenyl)piperazine | HCID 1346 | — |
| Reactant | N-((4-(chloromethyl)phenyl)methyl)acetamide | HCID 15550682 | — |
| Reactant | N-(4-(1-chloroethyl)phenylmethyl)acetamide | HCID 18423036 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18423158 | HCID 18423158 | — |
Reaction Steps
In Example 1(5), N-((4-(1-chloroethyl)phenyl)methyl)acetamide was used for reaction instead of N-(4-chloromethylphenylmethyl)acetamide and 1-(2-methoxyphenyl)piperazine instead of 1-phenylpiperazine, which was followed by treatment with 4M hydrochloric acid-dioxane in ethanol to give the title compound as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455528B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-0a331dc079e94ae49fdb1a05ea018a17 |
| Source note | uspto-grants-2002_09 |