1-(2-Pyridyl)piperazine → HCID 11645776, compound

HRID 1282201Notes

Reaction equation

HRID 1282201 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[N:7]1[CH2:12][CH2:11][NH:10][CH2:9][CH2:8]1.Cl[CH:14]([C:16]1[CH:21]=[CH:20][C:19]([CH2:22][NH:23][C:24](=[O:26])[CH3:25])=[CH:18][CH:17]=1)[CH3:15]>>[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[N:7]1[CH2:8][CH2:9][N:10]([CH:14]([C:16]2[CH:21]=[CH:20][C:19]([CH2:22][NH:23][C:24](=[O:26])[CH3:25])=[CH:18][CH:17]=2)[CH3:15])[CH2:11][CH2:12]1

Participants

3

Reactant 2

HCID 944591-(2-Pyridyl)piperazineHCID 18423036N-(4-(1-chloroethyl)phenylmethyl)acetamide

Product 1

HCID 11645776HCID 11645776, compound

Procedure

By similar reaction and treatment to that in Example 1(5) using 1-(2-pyridyl)piperazine instead of phenylpiperazine and N-(4-(1-chloroethyl)phenylmethyl)acetamide instead of N-(4-chloromethylphenylmethyl)acetamide, the title compound can be obtained.

Workup

  1. customBy similar reaction and treatment to that in Example

Sources & evidence

ORD record
ord-88b5d7bacf444613af4908de7efbf172
Source dataset
uspto-grants-2002_09
Patent number
US06455528B1

Reaction notes

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