HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-methylphenyl isothiocyanate → HCID 9815210, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-methylphenyl isothiocyanate | HCID 29519 | — |
| Reactant | 2-Amino-4,5-dimethyl-1,3-thiazole | HCID 73238 | — |
| Product | HCID 9815210 | HCID 9815210 | 31.4% |
Reaction Steps
Prepared using Method B from 4.5 g (24.5 mmol) of 5-chloro-2-methyl-phenyl isothiocyanate and 2.79 g (24.5 mmol) of 2-amino-4,5-dimethylthiazole to give 2.4 g of title compound as a white solid (31% yield, m.p. 188-189° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455566B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-f442c5de00c440adb6f16fecb12c7583 |
| Source note | uspto-grants-2002_09 |