HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3,5-trimethyl-1H-pyrazol-4-amine → HCID 9901233, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3,5-trimethyl-1H-pyrazol-4-amine | HCID 161603 | — |
| Reactant | 2-Chloro-6-Methylphenyl Isothiocyanate | HCID 3731725 | — |
| Product | HCID 9901233 | HCID 9901233 | 67% |
Reaction Steps
Prepared using Method A from 4.0 g (21.8 mmol) of 2-chloro-6-methyl-phenyl isothiocyanate and 2.7 g (21.8 mmol) of 4-amino-1,3,5-trimethylpyrazole to give 4.5 g of title compound as a white solid (67% yield, m.p. 201-202° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455566B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-4639d874d1f94592bd62c65824d0e039 |
| Source note | uspto-grants-2002_09 |